HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 59655886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | HCID 59655889 | HCID 59655889 | — |
| Product | HCID 59655886 | HCID 59655886 | 62% |
Reaction Steps
A solution of Example 84 Part D (22.6 mg, 0.066 mmol) in 2-aminoethanol (5 mL) was heated at 100° C. for 24 h. 2-aminoethanol was then removed under vacuum, and the residue was purified by prep-HPLC, furnishing the title compound (15 mg, 62% yield). ESI m/z=369.24 [(M+H)+; calcd for C18H20N6O3+H: 369.17].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329668B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-255411aee26d49708eefc592200e8d5a |
| Source note | uspto-grants-2008_02 |