Methanol → HCID 19364541, compound

HRID 2054570Notes

Reaction equation

HRID 2054570 reaction equation
C[Si](C)(C)[O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][NH:9][C:10](=[O:13])[CH:11]=[CH2:12].CO.C(C1C=C(C)C=C(C(C)(C)C)C=1O)(C)(C)C>C(O)(=O)C>[OH:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][NH:9][C:10](=[O:13])[CH:11]=[CH2:12]

Participants

5

Reactant 3

HCID 887MethanolHCID 314042,6-Di-tert-butyl-4-methylphenolHCID 85790982HCID 85790982, compound

Product 1

HCID 19364541HCID 19364541, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

N-[2-(2-trimethylsiloxyethoxy)ethyl]acrylamide (73.5 g), methanol (400 g) and acetic acid (50 g) were introduced into a 1 L eggplant type flask and were mixed to a homogeneous state, after which the mixture was allowed to stand at room temperature overnight. 2,6-di-t-butyl-4-methylphenol (0.2 g) was added, after which the solvent was removed by means of a rotary vacuum evaporator (using a vacuum pump; bath temperature, 60 to 70° C.). The volatile components were removed by means of a vacuum pump under decreased pressure over a two-hour period at 70° C. and N-[2-(2-hydroxyethoxy)ethyl]acrylamide was obtained as a yellow transparent, viscous liquid.

Workup

  1. additionwere mixed to a homogeneous state
  2. customafter which the solvent was removed by means of a rotary vacuum evaporator (
  3. customtemperature, 60 to 70° C.
  4. customThe volatile components were removed by means of a vacuum pump
  5. customat 70° C.

Sources & evidence

ORD record
ord-86309177f92546a1898392385a84b07d
Source dataset
uspto-grants-2008_02
Patent number
US07329694B2

Reaction notes

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