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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2054633Generated: October 30, 2026

1,3-Benzodioxol-5-amine → HCID 21938137, compound

https://huagongshe.com/reaction/2054633

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Benzodioxol-5-amineHCID 84310—
Reactant3-Fluoro-4-nitrophenolHCID 520948—
ProductHCID 21938137HCID 21938137—

Reaction Conditions

Temperature120 °C

Reaction Steps

0.86 g of 3-fluoro-4-nitrophenol and 2.25 g of 3,4-methylenedioxyaniline were mixed and stirred for 5 hours at 120° C. The raw mixture was chromatographed on silica gel.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07329679B2
Source datasetuspto-grants-2008_02
ORD IDord-7018a70f042149c7829108aa7afac760
Source noteuspto-grants-2008_02