HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21938005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21938066 | HCID 21938066 | — |
| Product | HCID 21938005 | HCID 21938005 | — |
Reaction Steps
24.9 g of N,N-dimethyl-N′-(5-chloro-2-nitrophenyl)benzene-1,4-diamine was added to a solution that consists of 8 g of sodium in 200 ml of methanol, and the mixture was heated in an autoclave for 9 hours to 120° C. After cooling, crystalline product was suctioned out.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329679B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-d0cbec159e544434aebe7f6b57d6e9b1 |
| Source note | uspto-grants-2008_02 |