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HRID2054667

反应详情

EQUATION

反应方程式

HRID 2054667 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N)cc1C
HCID7248

3,4-Dimethylaniline

C8H11N

结构：O=[N+]([O-])c1cc([N+](=O)[O-])c(F)cc1O
HCID15083885

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(Nc2cc(O)c([N+](=O)[O-])cc2[N+](=O)[O-])cc1C
HCID21938041

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

CONDITIONS

反应条件

温度
40 °C

PROCEDURE

实验过程

6.6 g of 3,4-dimethylaniline was added to a suspension that consists of 4 g of 4,6-dinitro-3-fluorophenol (J. Org. Chem. 1991, 5958) in 100 ml of ethanol, and it was stirred for 7 days at 40° C. After cooling, it was suctioned off, and the residue was recrystallized from ethanol.

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe residue was recrystallized from ethanol