Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxy-5-nitroquinoline → 2-Methoxyquinolin-5-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxy-5-nitroquinoline | HCID 21948893 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-Methoxyquinolin-5-amine | HCID 12283036 | — |
반응 단계
550 mg (2.7 mmol) of 2-methoxy-5-nitroquinoline is stirred in 15 ml of ethyl acetate in the presence of 138 mg of 10% Pd—C for 5 hours in a hydrogen atmosphere. The batch is filtered, and the filtrate is concentrated by evaporation: 520 mg of a light yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07329753B2 |
| 출처 데이터셋 | uspto-grants-2008_02 |
| ORD ID | ord-8bd84f8d7ead457f8b7238f922c55fa4 |
| 출처 메모 | uspto-grants-2008_02 |