HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 69196886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | (8Z)-8-Tetradecenal | HCID 6430188 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 69196886 | HCID 69196886 | — |
Reaction Steps
5.6 g (Z)-8-tetradecenal (6), 2.0 g ethylene glycol and 20 mg p-toluenesulphonic acid in 150 ml toluene were boiled in a water separator for 3 h. The reaction mixture was washed with sodium bisulphate solution and dried over sodium sulphate and the solvent was distilled off. Chromatography on silica gel gave 2-[(Z)-tridec-7-enyl]-1,3-dioxolane (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332468B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-012a671326b345ec82fce2e54ddf8180 |
| Source note | uspto-grants-2008_02 |