HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86606203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | [(2-Bromo-2-phenylethyl)sulfonyl]benzene | HCID 220653 | — |
| Reactant | 1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2) | HCID 23080512 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86606203 | HCID 86606203 | 99.6% |
Reaction Steps
A mixture of (2-benzenesulfonylmethyl)-benzyl bromide (0.5 g, 1.54 mmol), N-phenacyl piperazine dihydrochloride (0.32 g, 1.54 mmol) and K2CO3 (0.74 g, 5.38 mmol) in 40 ml of acetone was treated according to general preparation 2 to give 0.4 g of compound (IV-26), yield 50%. M+ 448.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332495B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-9193b9f93f974698a3ef5b4b2940c0ae |
| Source note | uspto-grants-2008_02 |