HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-iodopyridine → HCID 86759578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-iodopyridine | HCID 4397176 | — |
| Reactant | 1,1-Dimethylethyl N-[(3S,4S)-4-methyl-3-piperidinyl]carbamate | HCID 45092192 | — |
| Product | HCID 86759578 | HCID 86759578 | 20% |
Reaction Steps
The cis product from Example 39C (0.428 g, 2.00 mmol) and 2-chloro-5-iodopyridine (0.523 g, 2.19 mmol; Aldrich) were processed according to the procedure in Example 1A to provide the title compound (0.13 g, 20%). MS (CI/NH3) m/z 326/328 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332504B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-ab6af583d2fb41058181f7be15e548c2 |
| Source note | uspto-grants-2008_02 |