HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-iodopyridine → HCID 86759579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-iodopyridine | HCID 4397176 | — |
| Reactant | 1,1-Dimethylethyl N-[(3S,4S)-4-methyl-3-piperidinyl]carbamate | HCID 45092192 | — |
| Product | HCID 86759579 | HCID 86759579 | 24.4% |
Reaction Steps
The trans product from Example 39C (0.146 g, 0.68 mmol) and 2-chloro-5-iodopyridine (0.21 g, 0.88 mmol; Aldrich) were processed according to the procedure in Example 1A to provide the title compound (0.054 g, 24%). MS (CI/NH3) m/z 326/328 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332504B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-a37ee888955f47afb12a2f5171ad92f2 |
| Source note | uspto-grants-2008_02 |