反应详情

The title compound was prepared from ethyl 5-amino-1-benzyl-3-phenyl-1H-indole-2-carboxylate and 4-dibenzothiopheneboronic acid according to the procedure of Example 1 Step 3 as a black solid: 1H NMR (DMSO-d6) δ 5.82 (s, 2 H), 7.00-8.20 (m, 27 H); MS (ESI) m/z 525 (MH+); HRMS calcd. for C34H25N2O2S: 525.1637; found (ESI+): 525.1622; Anal. calcd. for C34H24N2O2S.0.3ACN: C, 74.88; H, 4.89; N, 5.81. Found: C, 75.14; H, 4.53; N, 5.82.