Tetrabutylammonium Fluoride → HCID 73176549, compound

HRID 2055837Notes

Reaction equation

C[Si](C)(C)[C:3]#[C:4][CH:5]=[CH:6][C:7]#[C:8][CH2:9][CH2:10][CH2:11][CH3:12].CCCC[N+](CCCC)(CCCC)CCCC.[F-]>>[CH:3]#[C:4][CH:5]=[CH:6][C:7]#[C:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

Reactant 2

HCID 2724141Tetrabutylammonium Fluoride

HCID 72741377HCID 72741377, compound

Product 1

HCID 73176549HCID 73176549, compoundYield 80%

Procedure

Treatment of compound (a5) from Example 5 with TBAF according Method C of the above-described General Synthesis Procedures I produced the title compound in 80% yield.

Sources & evidence

ORD record: ord-54cef6e58075449b91253d5131e1db59
Source dataset: uspto-grants-2008_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07332623B2

Reaction notes

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