HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-2,4-dichloro-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Reactant | Benzenesulfonyl chloride, 2,4-dichloro- | HCID 204419 | — |
| Product | N-(2-benzoyl-4-chloro-phenyl)-2,4-dichloro-benzenesulfonamide | HCID 11247683 | — |
Reaction Steps
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 123 mg of 2,4-dichloro-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 7.24 (m, 1H), 7.31 (m, 1H), 7.45 (m, 2H), 7.54 (m, 2H), 7.60-7.65 (m, 2H), 7.97 (d, 1H, J=8.4 Hz), 10.23 (s, 1H). MS: m/z 440.7 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07335653B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-37277de5b8af476b99fc560430201372 |
| Source note | uspto-grants-2008_02 |