HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2057150Generated: October 25, 2026
Triethyl Phosphate → HCID 178448396, compound
https://huagongshe.com/reaction/2057150
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl Phosphate | HCID 6535 | — |
| Reactant | HCID 178448397 | HCID 178448397 | — |
| Product | HCID 178448396 | HCID 178448396 | 91.5% |
Reaction Steps
A solution containing di-tert-butylphenyliodonium chloride (443 mg; 1 mmol) and triethyl phosphate (3 g) was stirred at 110-120° C. for 1 hour. The thus-obtained solid matter was washed with ether, to thereby yield 432 mg of the target compound as white crystals (yield: 69.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07335787B2 |
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| Source dataset | uspto-grants-2008_02 |
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| ORD ID | ord-15f3daffdce24f3580cd49b8d6e89d58 |
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| Source note | uspto-grants-2008_02 |
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