HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,7-Dibromoheptane → HCID 178486060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,7-Dibromoheptane | HCID 78309 | — |
| Reactant | HCID 178486055 | HCID 178486055 | — |
| Product | HCID 178486060 | HCID 178486060 | — |
Reaction Steps
In analogy to examples 1.4 and 1.5, trans-(4-Hydroxy-cyclohexyl)-methyl-carbamic acid tert-butyl ester was reacted with 1,7-dibromoheptane to yield trans-[4-(7-Bromo-heptyloxy)-cyclohexyl]-methyl-carbamic acid tert-butyl ester which was reacted with N-allylmethylamine to yield trans-(4-[7-(Allyl-methyl-amino)-heptyloxy]-cyclohexyl)-methyl-carbamic acid tert-butyl ester as colorless oil, MS: 397 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07335687B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-585e66ed6989465280b9662935367d1c |
| Source note | uspto-grants-2008_02 |