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HRID2057261

反应详情

EQUATION

反应方程式

HRID 2057261 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=O)Cl
HCID6598

Dimethylcarbamoyl chloride

C3H6ClNO

结构：CN(C(=O)OC(C)(C)C)[C@H]1CC[C@H](C=C(Br)Br)CC1
HCID178486027

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=O)C#C[C@H]1CC[C@H](N(C)C(=O)OC(C)(C)C)CC1
HCID178484536

未命名化合物

PROCEDURE

实验过程

In a similar way as described in example 26.5, trans-[4-(2,2-Dibromo-vinyl)-cyclohexyl]-methyl-carbamic acid tert-butyl ester and dimethylcarbamoyl chloride gave trans-(4-Dimethylcarbamoylethynyl-cyclohexyl)-methyl-carbamic acid tert-butyl ester, mp: 115-117° C.; MS: 309 (MH+).