HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178457208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | N-Methylallylamine | HCID 69391 | — |
| Reactant | 3,5-Difluorophenyl chloroformate | HCID 22567683 | — |
| Reactant | HCID 178484796 | HCID 178484796 | — |
| Product | HCID 178457208 | HCID 178457208 | — |
Reaction Steps
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.Trifluoroacetic acid salt and 3,5-difluoro-phenyl chloroformate were reacted, followed by treatment with N-allyl-N-methylamine to give trans-{4-[5-(Allyl-methyl-amino)-pentyl]-cyclohexyl}-methyl-carbamic acid 3,5-difluoro-phenyl ester, MS: 409 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07335687B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-62bc2953ef044ac1854de135524c1e6f |
| Source note | uspto-grants-2008_02 |