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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2057284Generated: October 26, 2026

Trifluoroacetic acid → HCID 178457206, compound

https://huagongshe.com/reaction/2057284

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantN-MethylpropylamineHCID 12315—
Reactant4-Chlorophenyl chloroformateHCID 139059—
ReactantHCID 178484796HCID 178484796—
ProductHCID 178457206HCID 178457206—

Reaction Steps

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.Trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with methyl-propyl-amine to give trans-Methyl-{4-[5-(methyl-propyl-amino)-pentyl]-cyclohexyl}-carbamic acid 4-chloro-phenyl ester, MS: 409 (MH+, 1Cl).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07335687B2
Source datasetuspto-grants-2008_02
ORD IDord-a94f37232e6c4a1da164728fabf79073
Source noteuspto-grants-2008_02