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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2057285Generated: October 26, 2026

Dimethylamine → HCID 178483432, compound

https://huagongshe.com/reaction/2057285

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantTrifluoroacetic acidHCID 6422—
Reactant4-Chlorophenyl chloroformateHCID 139059—
ReactantHCID 178484796HCID 178484796—
ProductHCID 178483432HCID 178483432—

Reaction Steps

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.Trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with dimethylamine to give trans-Methyl-{4-[5-(dimethylamino)-pentyl]-cyclohexyl}-carbamic acid 4-chloro-phenyl ester, MS: 381 (MH+, 1Cl).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07335687B2
Source datasetuspto-grants-2008_02
ORD IDord-ad18b6a6530d44fd891c353c568069ef
Source noteuspto-grants-2008_02