N-bromobutanimide → Silver bromide

HRID 2057434Notes

Reaction equation

HRID 2057434 reaction equation
[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Ag+:25].[Br:26]N1C(=O)CCC1=O>CC(C)=O>[Ag:25][Br:26].[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Ag+:25]

Participants

5

Reactant 2

HCID 67184N-bromobutanimideHCID 164971Silver behenate

Product 2

HCID 66199Silver bromideHCID 164971Silver behenate

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Then, the polymer dispersion of silver behenate was maintained at 50° C., and with stirring at 500 rpm, and acetone solution of N-bromosuccinimide (0.7 g of N-bromosuccinimide+50 ml of acetone) at 25° C. was added over the course of 90 minutes. The mixture was further stirred for 60 minutes to form a polymer dispersion of silver bromide and silver behenate.

Workup

  1. additionwas added over the course of 90 minutes

Sources & evidence

ORD record
ord-71b58e9ac3fd4a878f27d4c3e638acd0
Source dataset
uspto-grants-1980_07
Patent number
US04210711

Reaction notes

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