HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20231523, compound → 3,14-Diethylhexadecane-4,13-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20231523 | HCID 20231523 | — |
| Reactant | 3,12-Di-(3-pentyl)-1,2-diazacyclododecane | HCID 23455931 | — |
| Product | 3,14-Diethylhexadecane-4,13-diamine | HCID 20231520 | — |
Reaction Steps
The procedure described in (a) is repeated, starting from 49 g (0.16 mole) of 3,12-di-(3-pentyl)-1,2-diazacyclododecane and using correspondingly reduced amounts of catalyst and solvent, affording after purification by chromatography 37.5 g (75% of theory) of 4,13-diamino-3,14-diethylhexadecane as a colourless oil [nD20 =1.4664; IR spectrum (liquid) includes bands at 3330, 1626 cm-1 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04210742 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-1eb75c7d1502458abecfa46aa3476b71 |
| Source note | uspto-grants-1980_07 |