HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 20332402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | ethyl 1,5-dihydro-1,5-dioxo-4H-1-benzopyrano[3,4-b]-pyridine-2-carboxylate | HCID 12377591 | — |
| Product | HCID 20332402 | HCID 20332402 | 75.4% |
Reaction Steps
Prepared from ethyl 1,5-dihydro-1,5-dioxo-4H-1-benzopyrano[3,4-b]-pyridine-2-carboxylate (9.5 g, 0.033 mole) and ethyl iodide (20.8 g, 0.134 mole) by the method described for Ex. 6. Recrystallization from dimethylformamide gives white crystals (7.8 g, 75%), m.p. 180-181.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04210758 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-cb2f9a1b1bc44187a9f541e74f97ef06 |
| Source note | uspto-grants-1980_07 |