HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → Ethanone, 1-(4-amino-2-methyl-5-(3-methylphenyl)-1H-pyrrol-3-YL)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | α-Amino-3-methylbenzeneacetonitrile | HCID 12339418 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethanone, 1-(4-amino-2-methyl-5-(3-methylphenyl)-1H-pyrrol-3-YL)- | HCID 41886 | — |
Reaction Steps
Starting from 2-amino-2-(m-tolyl)acetonitrile and acetylacetone, the open-chain intermediate compound is obtained, b.p. 170° C./0.02 mm Hg. The title compound is obtained in a 59% overall yield, m.p. 195°-7° C. (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211708 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-bc1f82d616864604bb36847d445ecced |
| Source note | uspto-grants-1980_07 |