HCID 86736991, compound → HCID 86736991, compound

Participants

Reaction Steps

To a solution of 10.15 g (0.0351 mole) of Compound 1 in 200 ml H2O was added, with stirring and over a period of 30 minutes, a solution of 9.67 g (0.336 mole) ZnSO4.7H2O and 0.30 g (0.018 mole) MnSO4.7H2O dissolved in 25 ml H2O. The resulting precipitate was filtered, washed once with water and once with methanol, and dried under vacuum in a dessicator for 7 hours, to yield 10.8 g (96.5 percent of theory, calculated from Compound 1) of the titled compound as a fine purple powder.

Provenance & Evidence