HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 53852388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20331415 | HCID 20331415 | — |
| Product | HCID 53852388 | HCID 53852388 | — |
Reaction Steps
4-(3-phenoxypropoxy)phthalic acid (41 g; 0.134 mole) was refluxed for 30 minutes with excess acetic anhydride and the product evaporated to dryness in vacuo. Recrystallisation of the resulting white solid from ethyl acetate afforded material of m.p. 96°-98°. (Found; C, 68.48; H, 4.75; C17H14O5 requires; C, 68.45; H, 4.73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211791 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-fffff73b79cb41ebac6edfdcef85dffc |
| Source note | uspto-grants-1980_07 |