HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-[13-(4-Chlorophenyl)-12-tridecynylamino]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 4-[13-(4-chlorophenyl)-12-tridecylamino]benzoate | HCID 54279737 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-[13-(4-Chlorophenyl)-12-tridecynylamino]benzoic acid | HCID 20330969 | — |
Reaction Steps
A 4 g. sample of ethyl 4-[13-(4-chlorophenyl)-12-tridecylamino]benzoate is hydrolyzed with 1.6 g. 85% potassium hydroxide in 60 ml. 95% ethanol by refluxing the solution for 5 hours. The solution is cooled, diluted with 100 ml. water and acidified to pH 4.5 with 37% hydrochloric acid. The precipitate is collected, dried in vacuo and crystallized from acetone to yield the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211783 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-febc975e5be742cea81f97208dd0eb00 |
| Source note | uspto-grants-1980_07 |