HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → Ethyl 3-(4-acetamidophenyl)prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl 3-(4-aminophenyl)acrylate | HCID 97826 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | Ethyl 3-(4-acetamidophenyl)prop-2-enoate | HCID 53715054 | — |
Reaction Steps
A sample of 50 g. of ethyl p-aminocinnamate is dissolved in 500 ml. of ethyl ether and a solution of 28 g. of acetic anhydride in 30 ml. of ether is added dropwise. When the addition is complete, the reaction is allowed to stir for another hour. The mixture is then diluted with hexane and filtered, providing ethyl p-acetamidocinnamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211783 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-aef76b387ecd40e789ba34060c8ff656 |
| Source note | uspto-grants-1980_07 |