HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → Phosphonium, (10-carboxydecyl)triphenyl-, bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 11-Bromoundecanoic acid | HCID 17812 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Phosphonium, (10-carboxydecyl)triphenyl-, bromide | HCID 11432504 | — |
Reaction Steps
A solution of 81.4 g. 11-bromoundecanoic acid and 85.0 g. triphenylphosphine in 600 ml. acetonitrile is refluxed for 64 hours, then concentrated in vacuo. The resultant oil is dissolved in 200 ml. ether, whereupon crystals of the title compound form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211783 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-b53a4b0811bc4b86bd389f4244dd71ec |
| Source note | uspto-grants-1980_07 |