Phosphoric Acid → HCID 20540603, compound

HRID 2057697Notes

Reaction equation

HRID 2057697 reaction equation
[CH3:1][CH:2]([CH:8]=[CH2:9])[CH2:3][CH2:4][CH2:5][CH2:6][OH:7].P(=O)(O)(O)O>>[CH2:8]([C:2]1([CH3:1])[CH2:3][CH2:4][CH2:5][CH2:6][O:7]1)[CH3:9]

Participants

3

Reactant 2

HCID 1004Phosphoric AcidHCID 543351HCID 543351, compound

Product 1

HCID 20540603HCID 20540603, compound

Procedure

1.8 grams of 5-methyl-6-hepten-1-ol (containing 5.4 percent 5-methyl-5-hepten-1-ol and 2.4 percent impurities) was reacted with 18 cc of 85 percent phosphoric acid at room temperature for 3.5 hours. Then the solution was worked up using the procedure of Example II. The v.p.c. showed the following to be present:

Sources & evidence

ORD record
ord-bb803a036e57450d9e7249a82e041fc2
Source dataset
uspto-grants-1980_07
Patent number
US04212812

Reaction notes

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