HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → HCID 12789007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | HCID 12789002 | HCID 12789002 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 12789007 | HCID 12789007 | — |
| Product | HCID 20330051 | HCID 20330051 | — |
Reaction Steps
The 4-acetyl-3-benzylideneamino-1-(p-chlorobenzyl)-5-methyl-2-phenylpyrrole is prepared from the compound of Example 46 and p-chlorobenzyl chloride by procedure (a) of Example 49, m.p. 136°-137° C. (from ethanol/water). This compound is hydrolyzed as in procedure (b) of Example 49. Yield of the title compound: 58%, m.p. 164°-166° C. (from ethanol/water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04212806 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-99a5e973017d43d58bb945652e04d561 |
| Source note | uspto-grants-1980_07 |