HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 20330482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 20330526 | HCID 20330526 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20330482 | HCID 20330482 | — |
Reaction Steps
One equivalent of 2-methyl-3-acetoxy-4-formyl-5-acetoxymethylpyridine in 1 liter of anhydrous diethyl ether is treated with 1.5 equivalents of sodium borohydride and aged 3 hours at room temperature. The reaction mixture is quenched on excess aqueous ammonium chloride solution and the ether layer is separated. After magnesium sulfate drying, concentration in vacuo gives the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04212976 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-7f158fef73354df586300da3a9719517 |
| Source note | uspto-grants-1980_07 |