Ethyl xanthate → HCID 88781480, compound
Reaction equation
Cl[CH2:2][C:3]1[CH:8]=[N:7][C:6]([CH3:9])=[C:5]2[O:10][C:11](=[O:14])[O:12][CH2:13][C:4]=12.CCOC(S)=[S:19]>>[SH:19][CH2:2][C:3]1[CH:8]=[N:7][C:6]([CH3:9])=[C:5]2[O:10][C:11](=[O:14])[O:12][CH2:13][C:4]=12Participants
3
Procedure
5-Chloromethyl-8-methyl-2-oxo-4H-m-dioxino[4,5-c]pyridine is converted to the corresponding ethyl xanthogenate and reduced in accordance with the procedure of Example 19, Step B, to give 5-mercaptomethyl-8-methyl-2-oxo-4H-m-dioxino[4,5-c]pyridine.
Sources & evidence
- ORD record
- ord-47d2bd9dc32d4c7ea996cd06625abb99
- Source dataset
- uspto-grants-1980_07
- Patent number
- US04212976
Reaction notes
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