HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 4-fluoro-N-hydroxy- → alpha-p-chlorophenyl-N-p-fluorophenylnitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 4-fluoro-N-hydroxy- | HCID 164595 | — |
| Reactant | N-(4-Chlorobenzylidene)aniline | HCID 238776 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | alpha-p-chlorophenyl-N-p-fluorophenylnitrone | HCID 85976551 | — |
Reaction Steps
N-p-fluorophenylhydroxylamine (0.052 moles) was dissolved in ether (20 cc). This solution was treated with N-p-chlorobenzylideneaniline (0.05 moles) and dissolved in ether (50 cc). The product which separated was filtered and washed with ether to give α-p-chlorophenyl-N-p-fluorophenylnitrone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04214003 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-bcccf3d29c8340c4877bfff89a06d8b8 |
| Source note | uspto-grants-1980_07 |