HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 20298680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 20298677 | HCID 20298677 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20298680 | HCID 20298680 | 74.7% |
Reaction Steps
N-[[2-[3-(Dimethylamino)propoxy]-5-methoxyphenyl]-methylene]benzeneethanamine (39.5 g) is reduced with 13.0 g of sodium borohydride in 200 ml of methanol following the procedure described in Example 1C yielding 29.7 g of the title compound, boiling point 205°-210° C. at 0.4-0.5 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04214081 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-28ecc37fe8d643b7b4004c259f4c845f |
| Source note | uspto-grants-1980_07 |