HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 20298685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 4-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde | HCID 20298681 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20298685 | HCID 20298685 | 81.4% |
Reaction Steps
4-Methoxy-2-[3-(4-morpholinyl)propoxy]-benzaldehyde (29.7 g) and 13.0 g of phenethylamine are reacted in 110 ml of toluene following the procedure described in Example 1B, yielding 33.1 g of the title compound, boiling point 240°-245° C. at 0.1-0.2 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04214081 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-446a56bc67434624a584182a8adaf44c |
| Source note | uspto-grants-1980_07 |