HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → ethyl 2-[4-{N-(4-chlorophenyl)formimidoyl}phenoxy]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | Ethyl 2-(4-formylphenoxy)propionate | HCID 3016639 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | ethyl 2-[4-{N-(4-chlorophenyl)formimidoyl}phenoxy]propionate | HCID 14871451 | 94.8% |
Reaction Steps
(a) In 100 ml of dried benzene are dissolved 17.0 g of ethyl 2-(4-formylphenoxy)propionate and 9.73 g of 4-chloroaniline, and the mixture is refluxed under heating and with stirring for 6 hours. Concentration of the reaction mixture gives 24.0 g of ethyl 2-[4-{N-(4-chlorophenyl)formimidoyl}phenoxy]propionate as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04214094 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-277aef7aca204c249b5dec4be14fdf7b |
| Source note | uspto-grants-1980_07 |