HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl N-cyanodithioiminocarbonate → N-cyano-N'[2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| Reactant | 2-((2-Aminoethyl)thiomethyl)pyridine | HCID 12889401 | — |
| Product | N-cyano-N'[2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea | HCID 12889408 | — |
Reaction Steps
The reaction of 2-((2-aminoethyl)thiomethyl)pyridine with dimethylcyanodithioimidocarbonate by a method similar to that described in Example (3d) afforded N-cyano-N'-[2-(2-pyridylmethylthio)ethyl]-S-methylisothiourea, m.p. 85°-88°. (from isopropyl alcohol-ether) (Found: C, 49.6; H, 5.4; N, 21.0; S, 24.0% C11H14N4S2 requires: C, 49.6; H, 5.3; N, 21.0; S, 24.1%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04215125 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-ef8d0d6cb4ce456285e655d3cf762369 |
| Source note | uspto-grants-1980_07 |