HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-4-[(2-aminoethyl)thiomethyl]pyridine → HCID 178512223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-4-[(2-aminoethyl)thiomethyl]pyridine | HCID 23349965 | — |
| Reactant | N-benzoyl-N',N"-bis-[2-((3-bromo-2-pyridyl)methylthio)ethyl]guanidine | HCID 54262795 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178512223 | HCID 178512223 | — |
Reaction Steps
The reaction of 3-bromo-4-[(2-aminoethyl)thiomethyl]pyridine with N-benzoyl-bis-dimethylthioimidocarbonate in pyridine by the method described in Example 12 yielded N-benzoyl-N',N"-bis-[2-((3-bromo-2-pyridyl)methylthio)ethyl]guanidine which, on acid hydrolysis, yielded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04215125 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-9a57e04c66184fec8eb636c4bbfde326 |
| Source note | uspto-grants-1980_07 |