Potassium ethylxanthate → HCID 23350089, compound
Reaction equation
CCO[C:4]([S-])=[S:5].[K+].[NH2:8][C:9]1[C:14]([NH2:15])=[CH:13][C:12]([CH3:16])=[CH:11][C:10]=1[O:17][CH2:18][CH:19]([OH:25])[CH2:20][NH:21][CH:22]([CH3:24])[CH3:23]>>[OH:25][CH:19]([CH2:20][NH:21][CH:22]([CH3:23])[CH3:24])[CH2:18][O:17][C:10]1[C:9]2[NH:8][C:4](=[S:5])[NH:15][C:14]=2[CH:13]=[C:12]([CH3:16])[CH:11]=1Participants
3
Procedure
From potassium xanthogenate and 2,3-diamino-1-[2-hydroxy-3-(2-propylamino)-propoxy]-5-methylbenzene, using the process described in Example 3, there is obtained the title compound which, after recrystallisation from ethanol, decomposes at 294°-295° C.
Sources & evidence
- ORD record
- ord-ea28d99116a34adf8e6a378301910728
- Source dataset
- uspto-grants-1980_07
- Patent number
- US04215134
Reaction notes
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