Ethanol → HCID 23350101, compound

HRID 2058248Notes

Reaction equation

HRID 2058248 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]=[CH:11][NH:12][C:13]=2[C:14]2[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=2)=[CH:5][CH:4]=1.C(O)C>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[C:9]3[N:10]=[CH:11][NH:12][C:13]=3[C:14]3[C:19](=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=3)[C:7]=2[CH:8]=1

Participants

3

Reactant 2

HCID 702EthanolHCID 14100143HCID 14100143, compound

Product 1

HCID 23350101HCID 23350101, compound

Procedure

A solution of 4,5-bis(4-methoxyphenyl)imidazole in absolute ethanol[3.5 gms (0.0125 mole) in 800 ml absolute ethanol, 140 mg iodine as catalyst] was photolysed using a 450 watt Havovia lamp, and a Vycor filter for four hours.

Workup

  1. filtrationa Vycor filter for four hours

Sources & evidence

ORD record
ord-c9f8b9d58cf44c03b58c96f870dd9fe3
Source dataset
uspto-grants-1980_07
Patent number
US04215135

Reaction notes

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