Ethyl 2-chloroethylcarbamate → 2-[p-(p-Tert.butylphenoxy)phenoxy]ethylcarbamic acid ethyl ester

HRID 2058274Notes

Reaction equation

HRID 2058274 reaction equation
[CH3:1][C:2]([C:5]1[CH:18]=[CH:17][C:8]([O:9][C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)=[CH:7][CH:6]=1)([CH3:4])[CH3:3].[CH2:19]([O:21][C:22](=[O:27])[NH:23][CH2:24][CH2:25]Cl)[CH3:20]>>[CH2:19]([O:21][C:22](=[O:27])[NH:23][CH2:24][CH2:25][O:16][C:13]1[CH:12]=[CH:11][C:10]([O:9][C:8]2[CH:17]=[CH:18][C:5]([C:2]([CH3:1])([CH3:3])[CH3:4])=[CH:6][CH:7]=2)=[CH:15][CH:14]=1)[CH3:20]

Participants

3

Reactant 2

HCID 80621Ethyl 2-chloroethylcarbamateHCID 149712574-(4-tert-Butylphenoxy)phenol

Product 1

HCID 566364082-[p-(p-Tert.butylphenoxy)phenoxy]ethylcarbamic acid ethyl ester

Procedure

2-[p-(p-tert.butylphenoxy)phenoxy]ethylcarbamic acid ethyl ester as a yellow oil (nD20 =1.5436) is prepared from 4-[4-(1,1-dimethylethyl)phenoxy]phenol and (2-chloroethyl)carbamic acid ethyl ester.

Sources & evidence

ORD record
ord-067e88f456524a63a75ad751a639c68f
Source dataset
uspto-grants-1980_07
Patent number
US04215139

Reaction notes

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