Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2058439Generated: October 30, 2026

HCID 22819482, compound → HCID 86738273, compound

https://huagongshe.com/reaction/2058439

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22819482HCID 22819482—
ReactantHCID 178418287HCID 178418287—
ProductHCID 86738273HCID 86738273—

Reaction Steps

4-Diazo-17β-hydroxymethyl-5αandrostan-3-one is oxidized with pyridinium chlorochromate according to the procedure described in Example 4 to give 4-diazo-3-oxo-5α-androstane-17β-carboxaldehyde. In a similar manner, 4-diazo-17β-hydroxy-5α-androstan-3-one is oxidized with pyridinium chlorochromate to give 4-diazo-5α-androstane-3,17-dione.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04317817
Source datasetuspto-grants-1982_03
ORD IDord-e95cc6af9fb942dba90cf11b0a858fb7
Source noteuspto-grants-1982_03