化工社化工社 化学情報印刷レポート · 研究参考用
Fumaric Acid → 1-Cyclooctylmethylimidazole hydrogen fumarate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Fumaric Acid | HCID 444972 | — |
| 反応物 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Cyclooctylmethylimidazole hydrogen fumarate | HCID 20550237 | 71.9% |
反応手順
A solution of fumaric acid (0.22 g) in hot ethanol (10 ml) was added to a solution of 1 -cyclooctylmethyl imidazole (0.38 g) in ethanol (4 ml). After boiling for 10 minutes the solution was evaporated to afford a white solid. Recrystallisation from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen fumarate (0.42 g) as white needles, m.p. 147° to 148° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04317830 |
| 出典データセット | uspto-grants-1982_03 |
| ORD ID | ord-e96747ec888f4ddc9acd75a8341803fe |
| 出典メモ | uspto-grants-1982_03 |