Ammonia → HCID 178433312, compound

HRID 2058487Notes

Reaction equation

HRID 2058487 reaction equation
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2].[NH3:19]>>[N+:1]([CH:4]=[C:5]([NH2:19])[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 178503826HCID 178503826, compound

Product 1

HCID 178433312HCID 178433312, compound

Procedure

Reaction of 1-nitro-2-methylthio-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene (see Example 2(i)) with ammonia by the procedure of Example 2(ii) yields, after recrystallisation from methanol, the title compound, m.p. 193°-195° C.

Workup

  1. customyields
  2. customafter recrystallisation from methanol

Sources & evidence

ORD record
ord-c1a7adad9b4441ea995cbcfba41ddd06
Source dataset
uspto-grants-1982_03
Patent number
US04317829

Reaction notes

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