HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-En-1-Ol → (3-Phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-En-1-Ol | HCID 308 | — |
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | 3-Methylsalicylic Acid | HCID 6738 | — |
| Product | (3-Phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate | HCID 53972063 | 89.1% |
Reaction Steps
Using the method of example 1, 15.24 g of 2-hydroxy-3-methylbenzoic acid (0.1 moles), 40.251 g of 3-phenyl-2-propen-1-ol (0.3 moles) of 4.9 g of anhydrous phosphoric acid (0.05 moles) give 23.9 g (yield 89%) of (3-phenyl-2-propenyl)-2-hydroxy-3-methylbenzoate, m.p. 154°-154.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04317917 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-5506c82df35e45fdb6bb7a935ff9399e |
| Source note | uspto-grants-1982_03 |