HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylsalicylic Acid → HCID 54569622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylsalicylic Acid | HCID 6738 | — |
| Reactant | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 54569622 | HCID 54569622 | 81.8% |
Reaction Steps
Using the method of example 4, 14.815 g(0.1 moles) of 3-phenyl-2-propenoic acid and 20.82 g of SOCl2 (0.175 moles) followed by 15.24 g of 2-hydroxy-3-methylbenzoic acid (0.1 moles) give 23.1 g of 2-(3-phenyl-2-propenoyloxy)-3-methylbenzoic acid (yield 81.8%), m.p. 141°-141.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04317917 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-1addba22e61e40ed95f1e0cdf85ceb4e |
| Source note | uspto-grants-1982_03 |