Diethyl Sulfate → 2-Ethoxyethyl-cyclohexyl-ether

HRID 2058556Notes

Reaction equation

[OH:1][CH2:2][CH2:3][O:4][CH:5]1[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1.S(OCC)(O[CH2:15][CH3:16])(=O)=O>>[CH2:15]([O:1][CH2:2][CH2:3][O:4][CH:5]1[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1)[CH3:16]

Participants

Reactant 2

HCID 6163Diethyl Sulfate

HCID 2247752-(Cyclohexyloxy)ethanol

Product 1

HCID 198045672-Ethoxyethyl-cyclohexyl-ether

Procedure

The 2-ethoxyethyl-cyclohexyl-ether was prepared in correspondence with the description of Example 1 from 72 g (0.5 mol) of 2-hydroxyethyl-cyclohexyl-ether and 54 g (0.35 mol) of diethyl sulfate.

Sources & evidence

ORD record: ord-94427d6ca1ea42089862375c94f17a56
Source dataset: uspto-grants-1982_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04317942

Reaction notes

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