HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 20549424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 20549430 | HCID 20549430 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 20549424 | HCID 20549424 | — |
Reaction Steps
To 36.0 g (0.134 mols) 2,6-dichlorophenyl acetyl bromide, are added in drops at 160 degrees C., 21.5 g (0.134 mols) bromine over 3 hours, and the resultant mixture is then stirred for another 2 hours at 170 degrees C. While stirring, 100 ml hexane are added at 90 degrees C., followed by suction-filtering of the bromide after cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04318915 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-f9889921b20c4fb086272776f4a57aed |
| Source note | uspto-grants-1982_03 |