HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → 3-Benzylaminoacrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Benzylaminoacrylonitrile | HCID 70548701 | 72.1% |
Reaction Steps
9.7 g (0.1 mol) of 3-EAN and 21.4 g (0.2 mol) of benzylamine are refluxed for 4 h with removal of ethanol by distillation. Subsequent vacuum distillation yields 11.4 g of 3-benzylaminoacrylonitrile (72% with respect to 3-EAN).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319024 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-c179ea1549da4dd3b03926fca0d158d9 |
| Source note | uspto-grants-1982_03 |