HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | HCID 12670626 | HCID 12670626 | — |
| Product | HCID 13037518 | HCID 13037518 | 26% |
Reaction Steps
The procedure of Example 38 was employed utilizing N-benzylaniline and 3-methylphenyl phosphonic dichloride to yield 1-(3-methylphenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (2.5 g, 26% yield) as a white solid having a melting point of 155°-156° C., and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-938920b589a44ec0ac09b23305a4ee0e |
| Source note | uspto-grants-1982_03 |